Customization: | Available |
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CAS No.: | 616 45 5 |
Formula: | C4h7no |
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preparation
Production of 2-pyrrolidon by hydrocyanc acid and acrylonitril Hydrocanic acid (HCN) reacts with acrylonitril (AN) to prepare 2-pyrrolidon,
The reaction process is:
1) The addition reaction of HCN and AN is catalyzed by triethylamin to generate succinonitrile. The reaction was carried out at atmospheric pressure and about 70°C, and the yield of succinonitrile was as high as 97%.
2) Partial hydrogenation reduction of succinonitrile to aminobutyronitrile, reaction Chemicalbook uses carrier nickel as hydrogenation catalyst, total pressure 14.0MPa, temperature 80~100ºC, using liquid ammoni as solvent, succinonitrile conversion rate is close to 100%, The selectivity of aminobutyronitrile is 85%.
3) γ-aminobutyronitrile hydrolysis and cyclization reaction generates 2-pyrrolidon. This reaction is carried out in a plug flow system at a temperature of 210 °C, and the nitrile conversion rate and product selectivity are both close to 100%.
Dalian Sinobio Chemistry Co.,Ltd_was established in 2011 and located in beautiful costal city Dailan Liaoning Province. we can enjoy convenient transportation by all logistic ways. Sinobio cooperated with Dalian university of technology, who has 2 production sites: one located in Lanzhou city , Gan Su province who mainly produce biocides and pharmaceutical related. Another located in Fuzhou city,Jiangxi province .It was founded in 2013 with abundant financial resources.
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